2024

F. Merlo, F. Colucci, G. De Soricellis, F. Rinaldi, E. Calleri, A. Profumo, A. Speltini

Carbon nanotubes in high internal phase emulsion polymer composite for packed-cartridge micro-solid-phase extraction of fluoroquinolones in urine

Advances in Sample Preparation, 2024, 9, 100103

https://doi.org/10.1016/j.sampre.2024.100103

D. Merli, E. Lio, S. Protti, R. Coccia, A. Profumo, G. Alberti

Molecularly Imprinted Polymer-based voltammetric sensor for aminoacids/indazole derivatives synthetic cannabinoids detection

ACA, 2024, 1288, 342151

https://doi.org/10.1016/j.aca2023.342151

2023

F. Merlo, P. Bianchini, F. Maraschi, A. Speltini, A. Profumo

Pipette-tip μSPE coupled with HPLC-MS/MS for trace determination of fluoroquinolones in human urine

Talanta Open, 2023, 8, 100271

https://doi.org/10.1016/j.talo.2023.100271

F. Merlo, A. Profumo, A. Speltini

Sample treatment for the determination of steroid hormone contaminants in water samples: Analytical greenness assessment

TrAC – Trends in Analytical Chemistry, 2023, 169, 117393

https://doi.org/10.1016/j.trac.2023.117393

A. Speltini, F. Merlo, F. Maraschi, P. Bianchini, A. Mandri, A. Profumo

Multiclass ultrasound-assisted extraction, clean-up and high performance liquid chromatography-tandem mass spectrometry quantification of steroid hormone residues in compost

Journal of Chromatography A 1694 (2023) 463900

https://doi.org/10.1016/j.chroma.2023.463900

P. Bianchini, F. Merlo, F. Maraschi, R. Brescia, M. Prato, A. Profumo, A. Speltini

From Rice Husk Ash to Silica-Supported Carbon Nanomaterials: Characterization and Analytical Application for Pre-Concentration of Steroid Hormones from Environmental Waters.

Molecules 28 (2023) 745

https://www.mdpi.com/1420-3049/28/2/745

I. Quintanilla, C. Perelló, F. Merlo, A. Profumo, C. Fontàs, E. Anticó

Multiwalled Carbon Nanotubes Embedded in a Polymeric Matrix As a New Material for Thin Film Microextraction (TFME) in Organic Pollutant Monitoring.

Polymers 15 (2023) 314

https://www.mdpi.com/2073-4360/15/2/314

A. Speltini, G. Alberti, R. Rovida, C. Milanese, G. De Soricellis, F. Rinaldi, G. Massolini, A. Gallo, E. Calleri

Synthesis, characterization and application of a MIP-polyHIPE for selective extraction of angiotensin II receptor antagonists residues in natural waters

Int. J. Environ. Res. Public Health 2023, 20, 4878

https://doi.org/10.3390/ijerph20064878

L. Ferrari, A. Speltini

Neonicotinoids: an overview of the newest sample preparation procedures of environmental, biological and food matrices

Adv. Sample Prep. 2023, 8, 100094

https://doi.org/10.1016/j.sampre.2023.100094

2022

F. Merlo, D. Centenaro, F. Maraschi, A. Profumo, A. Speltini*

Green and Efficient Determination of Fluoroquinolone Residues in Edible Green Fruits and Leafy Vegetables by Ultrasound-Assisted Extraction Followed by HPLC-MS/MS.

Molecules 27 (2022) 6595

https://www.mdpi.com/1420-3049/27/19/6595

F. Merlo, J. Montagna, F. Maraschi, A. Profumo, F. Baldanti, A. Speltini

A versatile method for multiclass determination of β-lactam drugs in urine by solid-phase extraction followed by HILIC-UV.

Journal of Chromatography Open 2 (2022) 100048

https://doi.org/10.1016/j.jcoa.2022.100048

F. Merlo, A. Profumo, C. Fontas, E. Anticò

Preparation of new polymeric phases for thin-film liquid phase microextraction (TF-LPME) of selected organic pollutants.

Microchemical Journal 175 (2022) 107120

https://doi.org/10.1016/j.microc.2021.107120

F. Merlo, S. Suppini, F. Maraschi, A. Profumo, A. Speltini

A simple and fast multiclass method for determination of steroid hormones in berry fruits, root and leafy vegetables.

Talanta Open 5 (2022) 100081

https://doi.org/10.1016/j.talo.2021.100081

A. Speltini, G. Tripodo, F. Rinaldi, G. Massolini, A. Profumo, E. Calleri

Carbon nanotubes-modified poly-High Internal Phase Emulsions for pharmaceuticals pre-concentration and determination

Pharm. Biomed. Anal. 2022, 207, 114391

https://doi.org/10.1016/j.jpba.2021.114391

2021

A. Speltini, F. Merlo, F. Maraschi, G. Marrubini, A. Faravelli, A. Profumo

Magnetic Micro-Solid-Phase Extraction Using a Novel Carbon-Based Composite Coupled with HPLC–MS/MS for Steroid Multiclass Determination in Human Plasma.

Molecules 26 (2021) 2061

https://doi.org/10.3390/molecules26072061

A. Speltini, F. Merlo, F. Maraschi, L. Villani, A. Profumo

HA-C@silica sorbent for simultaneous extraction and clean-up of steroids in human plasma followed by HPLC-MS/MS multiclass determination.

Talanta 221 (2021) 121496

https://doi.org/10.1016/j.talanta.2020.121496

S. Dugheri, D. Massi, N. Mucci, G. Marrubini, G. Cappelli, A. Speltini, M.C. Bonferoni,

Arcangeli

Exposure to airborne formaldehyde: sampling and analytical methods – A review

Trend. Environ. Anal. Chem. 2021, 29, e00116

https://doi.org/10.1016/j.teac.2021.e00116

2020

F. Merlo, F. Maraschi, D. Piparo, A. Profumo, A. Speltini

Simultaneous Pre-concentration and HPLC-MS/MS Quantification of Phycotoxins and Cyanotoxins in Inland and Coastal Waters

Int. J. Environ. Res. Public Health 17 (2020) 4782

https://doi.org/10.3390/ijerph17134782

F. Merlo, A. Speltini, F. Maraschi, M. Sturini, A. Profumo

HPLC-MS/MS multiclass determination of steroid hormones in environmental waters after preconcentration on the carbonaceous sorbent HA-C@silica

Arabian Journal of Chemistry 13 (2020) 4673-4680

https://doi.org/10.1016/j.arabjc.2019.10.009

S. Dugheri, G. Marrubini, A. Speltini, N. Mucci, G. Cappelli, G. Bartolucci, G. Arcangeli

Fully automated determination of trimellitic anhydride in saturated polyester resins using programmed temperature vaporization-large volume injection-gas chromatography previous aqueous derivatization with triethyloxonium tetrafluoroborate

Chromatographia 2020, 83, 601-613

https://doi.org/10.1007/s10337-020-03877-0

G. Marrubini, S. Dugheri, G. Cappelli, G. Arcangeli, N. Muzzi, P. Appelblad, C. Melzi, A. Speltini

Experimental designs for solid-phase microextraction method development in bioanalysis: a review

Anal. Chim. Acta 2020, 1119, 77-100

https://doi.org/10.1016/j.aca.2020.04.012